SFTIR-530
FTIR Spectrometer
Stalwart has launched a new type FTIR Spectrometer SFTIR-530 with fully independent intellectual property rights. adhering to consistent excellent quality and superior performance, the new model obtains the best balance between intelligence and convenient operation, advance performance and low operation and maintenance cost. It is a good choice for basic science research analysis, produc
Quantity :
  • Features
  • Specifications
  • Accessories
  • Literature

Features

High Sensitivity Optical System

Cube-corner Michelson interferometer combined with patented fixing mirror alignment technology (Utility model ZL 2013

20099730.2: fixing mirror alignment assembly) , to ensure long term stability, without the need of dynamic alignment which

needs extra complicated electronic circuits. Reflecting mirrors are coated with gold to provide the maximum light

throughput and ensure the detection sensitivity.

High stability modular partition design

Compact structure modular design with layout on cast aluminum base and overall balance of mechanical robustness and partition heat dissipation, offering higher ability of deformation resistance and less sensitive to vibrations and thermal variations, greatly improves the mechanical stability and long-term working stability of the instrument.

Intelligent multi-sealed moisture-proof design

Multiple sealed interferometers, large-capacity desiccant cartridge with visible window and easy replacement structure, real-time monitoring of temperature and humidity inside the interferometer, getting rid of influences of high temperature, high humidity, and chemical corrosion to the optical system in many ways.

Innovated integration electronic system

High sensitivity pyroelectric detector pre-amplifier technology, dynamic gain amplification technology, high precision 24-bit A/D conversion technology, real-

Specifications

Interferometer

Cube-corner Michelson interferometer

Beam splitter

Multilayer Ge coated KBr

Detector

High sensitivity pyroelectric module (standard)

MCT detector (optional)

IR Source

High intensity, long lifetime, air-cooled IR source

Wavenumber Range

7800cm-1~350cm-1

Resolution

0.85 cm-1

Signal to noise ratio

ST-FTIR Better than 20,000:1 (RMS value, at 2100cm-1 ~ 2200cm-1, resolution: 4cm-1, 1 minute data collection)

ST-FTIR Pro: Better than 40,000:1 (RMS value, at 2100cm-1 ~ 2200cm-1, resolution: 4cm-1, 1 minute data collection)

Wavenumber Accuracy

±0.01 cm-1

Scanning Speed

Microprocessor control, different scanning speed selectable.

Software

MainFTOS Suite software workstation, compatible to all version Windows OS

FDA 21 CFR Part11 compliance software (optional)

Interface

Ethernet & WIFI wireless

Data Output

Standard data format, report generation and output

Status Diagnosis

Power on self-check, real-time temperature and humidity monitoring and reminders

Certification

CE

IQ/OQ/PQ(optional)

Environment Conditions

Temperature: 10℃~30℃,humidity: less than 60%

Power Supply

AC220V±22V,50Hz±1Hz/  AC110V(optional)

Dimensions & Weight

490×420×240 mm, 23.2kg

Accessories

Transmission sample holder (Standard)

Optional accessories such as gas cell, liquid cell, Defused/Specular Reflection, single/multiple reflection ATR, IR Microscope etc.

 

Accessories

Single Reflection ATR
Single reflection ATR can be used to measure various forms samples (liquid, viscous material, soft and ductile film and solid), and it has good results when testing substances with relatively strong absorption.


Horizontal ATR
A multi-reflection horizontal ATR can be used for the infrared analysis of solids, liquids, pastes and gels.
6-reflection and interchangeable sampling top plates(Specac) 12-reflection and integrated groove shape plate(Stalwart) Crystal materials: ZnSe


Single reflection ATR (Stalwart) Crystal materials: ZnSe

Single reflection ATR (Specac)
Crystal materials: Diamond, ZnSe and Ge

Horizontal ATR (Specac) Horizontal ATR (Stalwart)

Diffuse/Specular Reflectance Accessory
Diffuse/Specular reflectance accessory is a versatile diffuse reflectance and specular reflectance accessory. Diffuse reflection mode is used for transparent and powder sample analysis. Specular reflection mode is for measuring smooth reflective surface and coating surface.

• High light throughput

• Small light spot, able to measure micro samples

• Easy operation, no internal adjustment needed • Variable angle of incidence

• Optical aberration compensation

• Fast change of powder cup


Specular Reflection Accessory
Specular reflection accessory is fixed 10-degree angle of incidence. At a near-normal angle, the polarization effects on reflectivity are minimized. Specular reflection accessory is recommended to measure the reflectivity of glass. However, it may also be used to measure near-normal reflectivity of a wide variety of surfaces including military devices, reflecting optics, anti-reflective (AR) coated surfaces, and other reflecting and non-reflecting materials.
• Fixed 10-degree angle of incidence

 

Transmission Sample Clamp
Transmission sample clamp can be used to keep in place films, salt plates, KBr pellets and other materials.
• Clear aperture of the holder: 13 mm


Gas Cell
Gas cell is suitable for the detection of gas samples.
• Optional window plate: ZnSe and KBr
• Optional pathlength: 50 mm and 100 mm

Sealed Liquid Cell
Sealed liquid cell is usually used for qualitative or quantitative analysis of volatile liquids.
• Size of window:41x23x4 mm
• Optional window plates:KBr, CaF2 and ZnSe
• Optional pathlength: 0.05 mm, 0.1 mm, 0.2 mm, 0.5 mm and 1 mm.
• The standard pathlength is 0.5 mm


Demountable Liquid Cell
Demountable liquid cell is usually used for qualitative or quantitative analysis of non-volatile liquid sample.
• Size of window:25x4 mm
• Optional window plates:KBr, CaF2 and ZnSe
• Standard spacers include 0.05, 0.1, 0.2, 0.3, 0.5 and 1mm

Hydraulic Press 15T
The hydraulic press is for making high-quality KBr pellets for transmission FTIR analysis. The pellet preparation involves loading of the powdered KBr and sample matrix into the die chamber and placing the assembled die onto the platform of the hydraulic press.
• Clamp force, max 15 tons
• Diameter of die set: 13 mm

The TGA/FTIR Accessory
The TGA/FTIR accessory is designed to be an interface for evolved gas analysis from a thermogravimetric analyzer (TGA) to the FTIR spectrometer. Qualitative measurements is doable from sample masses, typically in the low milligram range.
• Gas cell pathlength: 100mm
• Gas cell volume: 38.5mL
• Temperature range of gas Cell: Room temp.~300℃
• Temperature range of transfer line: Room temp.~220℃
• Accuracy of temperature control: ±1℃
IR Microscope
IR microscope can be used in combination with FTIR spectrometer for high sensitivity detection of trace materials, infrared trace analysis and microanalysis, and apply to foreign bodies in drug component identification, drug analysis, drug packaging material of each component and the analysis of the foreign body.

Intelligent Electronic Moisture-proof Box
The intelligent electronic moisture-proof box adopts high-performance electronic dehumidification core and microcomputer humidity control, which has the characteristics of energy saving,
no noise, and intuitive display of humidity. The service life of the core components of the Fourier transform infrared spectrometer is longer.
• Humidity setting and control
• Temperature display
• Humidity over limit alarm


IR Oven
The IR oven as FTIR spectrophotometer accessory, mainly used for drying potassium bromide powder or window, silica gel and other easy delixidation materials, which can effectively improve the surface quality of the sample.
 

 

Literature

FTIR.pdf

Features

High Sensitivity Optical System

Cube-corner Michelson interferometer combined with patented fixing mirror alignment technology (Utility model ZL 2013

20099730.2: fixing mirror alignment assembly) , to ensure long term stability, without the need of dynamic alignment which

needs extra complicated electronic circuits. Reflecting mirrors are coated with gold to provide the maximum light

throughput and ensure the detection sensitivity.

High stability modular partition design

Compact structure modular design with layout on cast aluminum base and overall balance of mechanical robustness and partition heat dissipation, offering higher ability of deformation resistance and less sensitive to vibrations and thermal variations, greatly improves the mechanical stability and long-term working stability of the instrument.

Intelligent multi-sealed moisture-proof design

Multiple sealed interferometers, large-capacity desiccant cartridge with visible window and easy replacement structure, real-time monitoring of temperature and humidity inside the interferometer, getting rid of influences of high temperature, high humidity, and chemical corrosion to the optical system in many ways.

Innovated integration electronic system

High sensitivity pyroelectric detector pre-amplifier technology, dynamic gain amplification technology, high precision 24-bit A/D conversion technology, real-

Specifications

Interferometer

Cube-corner Michelson interferometer

Beam splitter

Multilayer Ge coated KBr

Detector

High sensitivity pyroelectric module (standard)

MCT detector (optional)

IR Source

High intensity, long lifetime, air-cooled IR source

Wavenumber Range

7800cm-1~350cm-1

Resolution

0.85 cm-1

Signal to noise ratio

ST-FTIR Better than 20,000:1 (RMS value, at 2100cm-1 ~ 2200cm-1, resolution: 4cm-1, 1 minute data collection)

ST-FTIR Pro: Better than 40,000:1 (RMS value, at 2100cm-1 ~ 2200cm-1, resolution: 4cm-1, 1 minute data collection)

Wavenumber Accuracy

±0.01 cm-1

Scanning Speed

Microprocessor control, different scanning speed selectable.

Software

MainFTOS Suite software workstation, compatible to all version Windows OS

FDA 21 CFR Part11 compliance software (optional)

Interface

Ethernet & WIFI wireless

Data Output

Standard data format, report generation and output

Status Diagnosis

Power on self-check, real-time temperature and humidity monitoring and reminders

Certification

CE

IQ/OQ/PQ(optional)

Environment Conditions

Temperature: 10℃~30℃,humidity: less than 60%

Power Supply

AC220V±22V,50Hz±1Hz/  AC110V(optional)

Dimensions & Weight

490×420×240 mm, 23.2kg

Accessories

Transmission sample holder (Standard)

Optional accessories such as gas cell, liquid cell, Defused/Specular Reflection, single/multiple reflection ATR, IR Microscope etc.

 

Accessories

Single Reflection ATR
Single reflection ATR can be used to measure various forms samples (liquid, viscous material, soft and ductile film and solid), and it has good results when testing substances with relatively strong absorption.


Horizontal ATR
A multi-reflection horizontal ATR can be used for the infrared analysis of solids, liquids, pastes and gels.
6-reflection and interchangeable sampling top plates(Specac) 12-reflection and integrated groove shape plate(Stalwart) Crystal materials: ZnSe


Single reflection ATR (Stalwart) Crystal materials: ZnSe

Single reflection ATR (Specac)
Crystal materials: Diamond, ZnSe and Ge

Horizontal ATR (Specac) Horizontal ATR (Stalwart)

Diffuse/Specular Reflectance Accessory
Diffuse/Specular reflectance accessory is a versatile diffuse reflectance and specular reflectance accessory. Diffuse reflection mode is used for transparent and powder sample analysis. Specular reflection mode is for measuring smooth reflective surface and coating surface.

• High light throughput

• Small light spot, able to measure micro samples

• Easy operation, no internal adjustment needed • Variable angle of incidence

• Optical aberration compensation

• Fast change of powder cup


Specular Reflection Accessory
Specular reflection accessory is fixed 10-degree angle of incidence. At a near-normal angle, the polarization effects on reflectivity are minimized. Specular reflection accessory is recommended to measure the reflectivity of glass. However, it may also be used to measure near-normal reflectivity of a wide variety of surfaces including military devices, reflecting optics, anti-reflective (AR) coated surfaces, and other reflecting and non-reflecting materials.
• Fixed 10-degree angle of incidence

 

Transmission Sample Clamp
Transmission sample clamp can be used to keep in place films, salt plates, KBr pellets and other materials.
• Clear aperture of the holder: 13 mm


Gas Cell
Gas cell is suitable for the detection of gas samples.
• Optional window plate: ZnSe and KBr
• Optional pathlength: 50 mm and 100 mm

Sealed Liquid Cell
Sealed liquid cell is usually used for qualitative or quantitative analysis of volatile liquids.
• Size of window:41x23x4 mm
• Optional window plates:KBr, CaF2 and ZnSe
• Optional pathlength: 0.05 mm, 0.1 mm, 0.2 mm, 0.5 mm and 1 mm.
• The standard pathlength is 0.5 mm


Demountable Liquid Cell
Demountable liquid cell is usually used for qualitative or quantitative analysis of non-volatile liquid sample.
• Size of window:25x4 mm
• Optional window plates:KBr, CaF2 and ZnSe
• Standard spacers include 0.05, 0.1, 0.2, 0.3, 0.5 and 1mm

Hydraulic Press 15T
The hydraulic press is for making high-quality KBr pellets for transmission FTIR analysis. The pellet preparation involves loading of the powdered KBr and sample matrix into the die chamber and placing the assembled die onto the platform of the hydraulic press.
• Clamp force, max 15 tons
• Diameter of die set: 13 mm

The TGA/FTIR Accessory
The TGA/FTIR accessory is designed to be an interface for evolved gas analysis from a thermogravimetric analyzer (TGA) to the FTIR spectrometer. Qualitative measurements is doable from sample masses, typically in the low milligram range.
• Gas cell pathlength: 100mm
• Gas cell volume: 38.5mL
• Temperature range of gas Cell: Room temp.~300℃
• Temperature range of transfer line: Room temp.~220℃
• Accuracy of temperature control: ±1℃
IR Microscope
IR microscope can be used in combination with FTIR spectrometer for high sensitivity detection of trace materials, infrared trace analysis and microanalysis, and apply to foreign bodies in drug component identification, drug analysis, drug packaging material of each component and the analysis of the foreign body.

Intelligent Electronic Moisture-proof Box
The intelligent electronic moisture-proof box adopts high-performance electronic dehumidification core and microcomputer humidity control, which has the characteristics of energy saving,
no noise, and intuitive display of humidity. The service life of the core components of the Fourier transform infrared spectrometer is longer.
• Humidity setting and control
• Temperature display
• Humidity over limit alarm


IR Oven
The IR oven as FTIR spectrophotometer accessory, mainly used for drying potassium bromide powder or window, silica gel and other easy delixidation materials, which can effectively improve the surface quality of the sample.
 

 

Literature

FTIR.pdf

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